HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,5-Diazabicyclo(4.3.0)non-5-ene → HCID 86743063, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,5-Diazabicyclo(4.3.0)non-5-ene | HCID 76349 | — |
| Reactant | Magnesium Chloride | HCID 5360315 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 86743063 | HCID 86743063 | 75.1% |
Reaction Steps
124.2 g (1.0 mole) of DBN and 47.6 g (0.5 moles) of anhydrous MgCl2 were refluxed in 250 g of acetone with heating for 10 hours, and then cooled. The deposited crystals were recovered therefrom by filtration, washed with acetone and dried, whereby 129.0 g of DBN/MgCl2 complex compound was obtained (yield: 75.1%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04833212 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-995c7f7150214ca58cfe78e42806c515 |
| Source note | uspto-grants-1989_05 |