HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium ethanethiolate → ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-thiocarboximidate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium ethanethiolate | HCID 4459711 | — |
| Reactant | 5,7-dihydro-6H-dibenz[c,e]azepine-6carbonitrile | HCID 19833886 | — |
| Solvent | Ethanethiol | HCID 6343 | — |
| Product | ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-thiocarboximidate | HCID 20041719 | — |
Reaction Steps
starting from 5,7-dihydro-6H-dibenz[c,e]azepine-6-carbonitrile and sodium ethanethiolate in ethanethiol there is obtained ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-thiocarboximidate and therefrom with hydrochloric acid in alcohol there is obtained the hydrochloride, m.p. 220° C. (with decomposition);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04833245 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-3da4a351d8e64400a8b8ced28462530c |
| Source note | uspto-grants-1989_05 |