HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → isopropyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 5,7-dihydro-6H-dibenz[c,e]azepine-6carbonitrile | HCID 19833886 | — |
| Product | isopropyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate | HCID 19833908 | — |
Reaction Steps
starting from 5,7-dihydro-6H-dibenz[c,e]azepine-6-carbonitrile and sodium isopropylate in isopropanol there is obtained isopropyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate and therefrom with hydrochloric acid in alcohol there is obtained the hydrochloride, m.p. 158° C. (with decomposition);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04833245 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-2b357e54a8be41818eceef318e8e1ccf |
| Source note | uspto-grants-1989_05 |