HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Alcohol → Benzyl 3,3-dimethylpent-4-enoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Alcohol | HCID 244 | — |
| Reactant | Ethyl 3,3-dimethylpent-4-enoate | HCID 82262 | — |
| Reactant | Sodium ethoxide | HCID 2723922 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Benzyl 3,3-dimethylpent-4-enoate | HCID 13236797 | 65% |
Reaction Steps
In the manner of Example I B, 810 mg of benzyl alcohol was reacted with 1122 mg of ethyl 3,3-dimethyl-4-pentenoate in the presence of 48 mg of sodium ethoxide in 30 ml of toluene to give 1.0 g (65% yield) of benzyl 3,3-dimethyl-4-pentenoate, b.p. 92°-98°/0.1 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04833266 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-3e7fd6ea5f304c2ba94d340494ccb2ea |
| Source note | uspto-grants-1989_05 |