HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4'-(1-Methyl-heptyloxy)-4-biphenylcarboxylic acid chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4'-(1-Methyl-heptyloxy)-4-biphenylcarboxylic acid | HCID 13643650 | — |
| Product | 4'-(1-Methyl-heptyloxy)-4-biphenylcarboxylic acid chloride | HCID 13643653 | 96.7% |
Reaction Steps
Thionyl chloride (11.3 g, 0.095 mol) was added to the above optically active 4'-(1-methyl-heptyloxy)-4-biphenylcarboxylic acid (20 g, 0.063 mol), followed by heating under reflux for one hour and distilling off excess thionyl chloride to obtain optically active 4'-(1-methyl-heptyloxy)-4-biphenylcarboxylic acid chloride (21 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04834907 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-c6eeed93a6184c99986565c1099522e9 |
| Source note | uspto-grants-1989_05 |