HCID 20039827, compound → HCID 20039825, compound

HRID 1762844Notes

Reaction equation

HRID 1762844 reaction equation
[CH3:1][N:2]1[CH:6]=[CH:5][N:4]=[C:3]1[N:7]1[CH2:12][CH2:11][CH:10]([C:13]2[CH:18]=[CH:17][C:16]([N+:19]([O-])=O)=[CH:15][CH:14]=2)[CH2:9][CH2:8]1.C(OCC)(=O)C.CCCCCC>CO>[NH2:19][C:16]1[CH:17]=[CH:18][C:13]([CH:10]2[CH2:9][CH2:8][N:7]([C:3]3[N:2]([CH3:1])[CH:6]=[CH:5][N:4]=3)[CH2:12][CH2:11]2)=[CH:14][CH:15]=1

Participants

4

Reactant 2

HCID 20039827HCID 20039827, compoundHCID 21226206Ethyl acetate hexane

Product 1

HCID 20039825HCID 20039825, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Hydrogenation of the product from part (iii) above (0.50 g) in methanol (30 ml) according to the method of Example 1(ii) gave the title compound, (0.43 g), m.p. 187°-188° from ethyl acetate/hexane.

Sources & evidence

ORD record
ord-082cd6692c6d4e9b96b5b94aa8050ea4
Source dataset
uspto-grants-1989_05
Patent number
US04835165

Reaction notes

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