HCID 20039828, compound → HCID 20039821, compound

HRID 1762845Notes

Reaction equation

HRID 1762845 reaction equation
[CH3:1][N:2]1[C:6]([CH3:7])=[CH:5][N:4]=[C:3]1[N:8]1[CH2:13][CH2:12][CH:11]([C:14]2[CH:19]=[CH:18][C:17]([N+:20]([O-])=O)=[CH:16][CH:15]=2)[CH2:10][CH2:9]1>CO>[NH2:20][C:17]1[CH:18]=[CH:19][C:14]([CH:11]2[CH2:10][CH2:9][N:8]([C:3]3[N:2]([CH3:1])[C:6]([CH3:7])=[CH:5][N:4]=3)[CH2:13][CH2:12]2)=[CH:15][CH:16]=1

Participants

3

Reactant 1

HCID 20039828HCID 20039828, compound

Product 1

HCID 20039821HCID 20039821, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Hydrogenation of the product from part (i) above (0.60 g) in methanol (50 ml) according to the method of Example 1(ii) gave the title compound, (0.53 g), m.p. 219°-220° (with decomp).

Sources & evidence

ORD record
ord-31d522985d6849fba79442dc1f682d0c
Source dataset
uspto-grants-1989_05
Patent number
US04835165

Reaction notes

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