Methanesulfonyl chloride → HCID 20039837, compound

HRID 1762846Notes

Reaction equation

HRID 1762846 reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]2[CH2:13][CH2:12][N:11]([C:14]3[N:15]([CH3:20])[C:16]([CH3:19])=[CH:17][N:18]=3)[CH2:10][CH2:9]2)=[CH:4][CH:3]=1.[CH3:21][S:22](Cl)(=[O:24])=[O:23]>N1C=CC=CC=1>[CH3:20][N:15]1[C:16]([CH3:19])=[CH:17][N:18]=[C:14]1[N:11]1[CH2:10][CH2:9][CH:8]([C:5]2[CH:6]=[CH:7][C:2]([NH:1][S:22]([CH3:21])(=[O:24])=[O:23])=[CH:3][CH:4]=2)[CH2:13][CH2:12]1

Participants

4

Reactant 2

HCID 31297Methanesulfonyl chlorideHCID 20039821HCID 20039821, compound

Product 1

HCID 20039837HCID 20039837, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

Treatment of the product from part (ii) above (0.46 g) with methanesulphonyl chloride (0.22 g) in pyridine (12 ml) according to the method fo Example 1(iii) gave the title compound, (0.40 g), m.p. 225°-226°.

Sources & evidence

ORD record
ord-1a0100c044804068aa3b408cba9e1fc3
Source dataset
uspto-grants-1989_05
Patent number
US04835165

Reaction notes

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