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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1762894Generated: October 30, 2026

HCID 14751596, compound → HCID 14751597, compound

https://huagongshe.com/reaction/1762894

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 14751596HCID 14751596—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 14751597HCID 14751597—

Reaction Steps

A solution of 1,6-dimethoxy-2,5-bis-[N-(cyclohexyl)benzyloxycarbonylaminomethyl)-naphthalene (250 mg) in methanol (10 ml) was hydrogenated at atmospheric pressure in the presence of 5% palladium-on-charcol (50 mg) for 2 hours at room temperature. The catalyst was removed by filtration through Celite, and the filtrate was evaporated to afford the product as a yellow syrup; yield 60 mg (37%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04835177
Source datasetuspto-grants-1989_05
ORD IDord-3d5b629b9b39444b80313e5b27b2b22c
Source noteuspto-grants-1989_05