HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14751596, compound → HCID 14751597, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14751596 | HCID 14751596 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 14751597 | HCID 14751597 | — |
Reaction Steps
A solution of 1,6-dimethoxy-2,5-bis-[N-(cyclohexyl)benzyloxycarbonylaminomethyl)-naphthalene (250 mg) in methanol (10 ml) was hydrogenated at atmospheric pressure in the presence of 5% palladium-on-charcol (50 mg) for 2 hours at room temperature. The catalyst was removed by filtration through Celite, and the filtrate was evaporated to afford the product as a yellow syrup; yield 60 mg (37%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04835177 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-3d5b629b9b39444b80313e5b27b2b22c |
| Source note | uspto-grants-1989_05 |