HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 70381823, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 13243449 | HCID 13243449 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 70381823 | HCID 70381823 | 189.4% |
Reaction Steps
617 mg of 7-benzyloxy-4-(N-benzyl-N-tert-butylaminoacetyl)-2-indolecarboxylic acid methoxymethyl ester is combined with 10 ml of methanol, 40 ml of absolute tetrahydrofuran, and 0.3 ml of acetic acid and hydrogenated and worked up as described in Example 31(E), thus obtaining 450 mg of 7-hydroxy-4-(1-hydroxy-2-tert-butylaminoethyl)indole-2-carboxylic acid methoxymethyl ester acetate, decomposition point 165°-170° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04835175 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-6bf43d92fe1148cf9b6098bc35ca703d |
| Source note | uspto-grants-1989_05 |