HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanethiol → HCID 14013757, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanethiol | HCID 6343 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 14013761 | HCID 14013761 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 14013757 | HCID 14013757 | 58.8% |
Reaction Steps
This material was prepared as described in Example 11: 3.36 g (0.009 mol) of product of Example 27, 0.86 g (0.006 mol) of K2CO3 and 12 ml (0.180 mol) of ethanethiol in 25 ml of acetone were reacted affording an orange oil which was kugelrohr distilled at 33 Pa, pot temperature 79° C. to give 2.11 g (58.8%) of product as a clear oil, nD25 1.4507.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04835279 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-e1a683ac3b61412cb9039519f7e2d1ee |
| Source note | uspto-grants-1989_05 |