HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 14013762, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 14013761 | HCID 14013761 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 14013762 | HCID 14013762 | 93.7% |
Reaction Steps
A mixture of 15.13 g (0.040 mol) of product of Example 27, 2.85 g (0.040 mol) of sodium azide and 175 ml of DMF was stirred for 1 hour and poured into 500 ml of water. The mixture was extracted with ether. The ether extract was washed several times with water, dried (MgSO4) and concentrated to give 14.4 g (93.7%) of product; mp 46°-47° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04835279 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-cd91e843a200404ebd1ae5ff19b6d766 |
| Source note | uspto-grants-1989_05 |