HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 14013838, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 14013807 | HCID 14013807 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 14013838 | HCID 14013838 | 59% |
Reaction Steps
This compound was prepared as described in Example 85: 17 g (0.264 mol) of zinc dust, 4.76 g (0.012 mol) of product of Example 56 and 17 ml of trifluoroacetic acid in 100 ml of CH2Cl2 were reacted affording 2.44 g (59%) of product after kugelrohr distillation at 100°-140° C./53 Pa as a light yellow oil, nD25 1.5032.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04835279 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-c838c1494643482b8f586467e6ccd77f |
| Source note | uspto-grants-1989_05 |