HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-((2-Nitrophenyl)azo)-4-(1,1,3,3-tetramethylbutyl)phenol → Octrizole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-((2-Nitrophenyl)azo)-4-(1,1,3,3-tetramethylbutyl)phenol | HCID 103927 | — |
| Reactant | 2-Nitro-2'-hydroxy-5'-t-butylazobenzene | HCID 135514582 | — |
| Product | Octrizole | HCID 62485 | 85.1% |
Reaction Steps
The same procedure as in Example 7 was repeated, except that 2-nitro-2'-hydroxy-5'-t-butylazobenzene 15.0 g was replaced by 2-nitro-2'-hydroxy-5'-t-octylazobenzene 17.7 g, thus producing 13.7 g of 2-(2'-hydroxy-5'-t-octylphenyl)benzotriazole having a melting point of 103° to 105° C. at the yield of 85.0%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04835284 |
| Source dataset | uspto-grants-1989_05 |
| ORD ID | ord-96f0c3208b2b40aabaef369f0ca9bed0 |
| Source note | uspto-grants-1989_05 |