HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → N-methyl-N-tert.-octylthiomethylamine hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1,3,5-Trimethyl-1,3,5-triazacyclohexane | HCID 7952 | — |
| Reactant | HCID 86735983 | HCID 86735983 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | N-methyl-N-tert.-octylthiomethylamine hydrochloride | HCID 85866484 | — |
Reaction Steps
300 ml. of acetonitrile, 12.9 g. (0.1 mole) of 1,3,5-trimethylhexahydro-s-triazine; 43.8 g. (0.3 mole) of tert.-octylthiomethylamine and 12 g. of hydrogen chloride gas are reacted together in the manner of Example I. A yield of 43.7 g. (64.6% of theory) of the title compound is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04111682 |
| Source dataset | uspto-grants-1978_09 |
| ORD ID | ord-dba2278fae3647809136087c4a36efe9 |
| Source note | uspto-grants-1978_09 |