Sulfuric Acid → HCID 20309632, compound

Participants

Reaction Steps

3-Glutarimido-5-nitrobenzoic Acid [D; Y is CH2CH2CH2, Z is OH] was prepared by heating a mixture of 18.2 g. of 3-amino-5-nitrobenzoic acid, 45.6 g. of glutaric anhydride and 0.5 ml. of concentrated sulfuric acid on a steam bath for 2 hours. The product was isolated and recrystallized from aqueous dimethylformamide to give 3-glutarimido-5-nitrobenzoic acid, pale yellow prisms, m.p. above 300° C.

Provenance & Evidence