Morpholine → HCID 20309613, compound

HRID 1763287Notes

Reaction equation

HRID 1763287 reaction equation
[NH2:1][C:2]1[C:3]([I:18])=[C:4]([C:8]([I:17])=[C:9]([N:12]([CH3:16])[C:13](=[O:15])[CH3:14])[C:10]=1[I:11])[C:5]([OH:7])=O.[NH:19]1[CH2:24][CH2:23][O:22][CH2:21][CH2:20]1>>[NH2:1][C:2]1[C:3]([I:18])=[C:4]([C:8]([I:17])=[C:9]([N:12]([CH3:16])[C:13](=[O:15])[CH3:14])[C:10]=1[I:11])[C:5]([N:19]1[CH2:24][CH2:23][O:22][CH2:21][CH2:20]1)=[O:7]

Participants

3

Reactant 2

HCID 8083MorpholineHCID 203096821949-42-4

Product 1

HCID 20309613HCID 20309613, compound

Procedure

4-[3-Amino-2,4,6-triiodo-5-(N-methylacetamido)benzoyl]morpholine [C; Ro is CH3CON(CH3), Q is H, Z is morpholino] was prepared from the acid chloride of 3-amino-5-(N-methylacetamido)-2,4,6-triiodobenzoic acid and morpholine according to the procedure described in Example 45, part (a). The product obtained was used directly in the procedure described in part (b) below.

Workup

  1. customThe product obtained

Sources & evidence

ORD record
ord-e3bcbc21d9404c7fb3fde9383721f7b4
Source dataset
uspto-grants-1978_09
Patent number
US04111937

Reaction notes

Loading…