Ethyl chloroformate → HCID 53753537, compound

HRID 1763294Notes

Reaction equation

[NH2:1][C:2]1[C:7]2[C:8]3[CH:9]=[N:10][CH:11]=[CH:12][C:13]=3[C:14]([CH3:17])([CH3:16])[O:15][C:6]=2[CH:5]=[C:4]([CH:18]([CH2:20][CH2:21][CH2:22][C:23]2[CH:28]=[CH:27][C:26]([F:29])=[CH:25][CH:24]=2)[CH3:19])[CH:3]=1.Cl[C:31]([O:33][CH2:34][CH3:35])=[O:32]>>[C:31]([NH:1][C:2]1[C:7]2[C:8]3[CH:9]=[N:10][CH:11]=[CH:12][C:13]=3[C:14]([CH3:17])([CH3:16])[O:15][C:6]=2[CH:5]=[C:4]([CH:18]([CH2:20][CH2:21][CH2:22][C:23]2[CH:24]=[CH:25][C:26]([F:29])=[CH:27][CH:28]=2)[CH3:19])[CH:3]=1)([O:33][CH2:34][CH3:35])=[O:32]

Participants

Reactant 2

HCID 10928Ethyl chloroformate

HCID 20309733HCID 20309733, compound

Product 1

HCID 53753537HCID 53753537, compound

Procedure

The title compound was prepared by reacting 10-amino-8-[5-(4-fluorophenyl)-2-pentyl]-5,5-dimethyl-5H-[1]benzopyrano[4,3-c]pyridine with ethyl chloroformate according to the method of Example 3.

Sources & evidence

ORD record: ord-eca4d9e13746479c83fe3a575e794a82
Source dataset: uspto-grants-1978_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04111942

Reaction notes

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