Chloranil → HCID 20309541, compound

HRID 1763323Notes

Reaction equation

HRID 1763323 reaction equation
[C:1]([NH:4][C:5]1[CH:6]=[CH:7][C:8]([O:18][CH2:19][CH:20]([OH:27])[CH2:21][NH:22][C:23]([CH3:26])([CH3:25])[CH3:24])=[C:9]([C:11]2[CH2:12][CH2:13][C:14](=[O:17])[NH:15][N:16]=2)[CH:10]=1)(=[O:3])[CH3:2].C1(Cl)C(=O)C(Cl)=C(Cl)C(=O)C=1Cl>C(O)CCC>[C:1]([NH:4][C:5]1[CH:6]=[CH:7][C:8]([O:18][CH2:19][CH:20]([OH:27])[CH2:21][NH:22][C:23]([CH3:26])([CH3:25])[CH3:24])=[C:9]([C:11]2[CH:12]=[CH:13][C:14](=[O:17])[NH:15][N:16]=2)[CH:10]=1)(=[O:3])[CH3:2]

Participants

4

Reactant 2

HCID 8371ChloranilHCID 20309483HCID 20309483, compound

Product 1

HCID 20309541HCID 20309541, compound

Reagents, catalysts & solvents 1

HCID 2631-ButanolSolvent

Procedure

6-[5-Acetamido-2-(3-t-butylamino-2-hydroxypropoxy)phenyl]-4,5-dihydro-3(2H)-pyridazinone was reacted with chloranil in boiling butanol to give 6-[5-acetamido-2-(3-t-butylamino-2-hydroxypropoxy)phenyl] -3(2H)-pyridazinone.

Sources & evidence

ORD record
ord-1e77caa7d77841ba848c7b0a21571970
Source dataset
uspto-grants-1978_09
Patent number
US04111936

Reaction notes

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