HuagongsheHuagongshe Chemistry Print Report · For research reference only
Epibromohydrin → HCID 20309580, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Epibromohydrin | HCID 18430 | — |
| Reactant | Propionic acid, 3-(6-hydroxy-m-anisoyl)-, methyl ester | HCID 143636 | — |
| Product | HCID 20309580 | HCID 20309580 | — |
Reaction Steps
Methyl 3-(2-hydroxy-5-methoxybenzoyl)propionate was reacted with epibromohydrin in a similar manner to that described in Example 1 (ii) to give methyl 3-[2-(2,3-epoxypropoxy)-5-methoxybenzoyl]propionate which, recrystallised from ether-petroleum ether (b.p. 60°-80°), had m.p. 50° - 51.5° C). (Found: C, 60.91; H, 6.07; C15H18O6 requires: C, 61.21; H, 6.17%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04111936 |
| Source dataset | uspto-grants-1978_09 |
| ORD ID | ord-4710d8d4b147449ab56e9c0261dbf134 |
| Source note | uspto-grants-1978_09 |