HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → Methyl 3-nitro-4-phenoxy-5-sulfamoylbenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 3-(Aminosulfonyl)-5-nitro-4-phenoxybenzoic acid | HCID 119926 | — |
| Product | Methyl 3-nitro-4-phenoxy-5-sulfamoylbenzoate | HCID 53854447 | — |
Reaction Steps
34 g (~0.1 mol) of 3-nitro-4-phenoxy-5-sulphamylbenzoic acid are dissolved in 150 ml of methanol and are heated to the boil. 5.4 ml of concentrated H2SO4 are then added slowly dropwise and the mixture is heated at reflux temperature for 10 hours. On cooling, 3-nitro-4-phenoxy-5-sulphamylbenzoic acid methyl ester crystallises.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04111953 |
| Source dataset | uspto-grants-1978_09 |
| ORD ID | ord-7daf1b8c5c2c4ef7a0c7d924767b14ec |
| Source note | uspto-grants-1978_09 |