反应详情

1.18 Grams (5.1 millimoles) of 1-bromotricyclo [4.3.1.12,5 ] undecane (X=Br in formula (II)) are dissolved in 10 ml of acetonitrile. The solution is cooled and kept at 0° C, and then 2.5 ml of concentrated sulfuric acid are added dropwise under stirring over 30 minutes. The stirring is continued further at room temperature for 20 hours. The reaction mixture is treated in the same manner as described in Example 1 to obtain 0.98 g (yield 92%) of 1-acetylaminotricyclo [4.3.1.12,5 ] undecane.

1. temperatureThe solution is cooled
2. customkept at 0° C
3. waitThe stirring is continued further at room temperature for 20 hours
4. additionThe reaction mixture is treated in the same manner