HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diglyme → HCID 13101068, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diglyme | HCID 8150 | — |
| Reactant | 4-Amino-2-[(diethylamino)methyl]phenol dihydrochloride | HCID 2723878 | — |
| Reactant | 3-chloro-2,1-benzothiazole | HCID 12210645 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 13101068 | HCID 13101068 | — |
Reaction Steps
Following a procedure similar to that described in Example 14 but reacting 10 g. of 3-chloro-2,1-benzisothiazole with 21 g. of 3-(diethylamino)methyl-4-hydroxyaniline dihydrochloride in 30 ml. of diglyme and 20 ml. of water there was obtained 3-{[3-(diethylamino)methyl-4-hydroxyphenyl]amino}-2,1-benzisothiazole, m.p. 164°-165° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04112105 |
| Source dataset | uspto-grants-1978_09 |
| ORD ID | ord-1e45aaf7be1f412d95e472206c50c627 |
| Source note | uspto-grants-1978_09 |