HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazinecarboxaldehyde → HCID 12726820, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazinecarboxaldehyde | HCID 12229 | — |
| Reactant | 3-Chloro-6-(2-fluorophenyl)pyridazine | HCID 12449555 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 12726820 | HCID 12726820 | — |
Reaction Steps
A mixture of 5.0 g. of 3-chloro-6-(o-fluorophenyl)pyridazine and 2.88 g. of formylhydrazine in 75 ml. n-butanol is refluxed for 48 hrs. and worked up as in Example 35 to give 1.1 g. of product as cream colored crystals, m.p. 161°-163° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04112095 |
| Source dataset | uspto-grants-1978_09 |
| ORD ID | ord-0e97792b25024b3fb1fabf37f03b5adc |
| Source note | uspto-grants-1978_09 |