Hydrazinecarboxaldehyde → HCID 12726819, compound

HRID 1763604Notes

Reaction equation

HRID 1763604 reaction equation
Cl[C:2]1[N:3]=[N:4][C:5]([C:8]2[CH:13]=[CH:12][CH:11]=[C:10]([F:14])[CH:9]=2)=[CH:6][CH:7]=1.[CH:15]([NH:17][NH2:18])=O>C(O)CCC>[F:14][C:10]1[CH:9]=[C:8]([C:5]2[CH:6]=[CH:7][C:2]3[N:3]([CH:15]=[N:17][N:18]=3)[N:4]=2)[CH:13]=[CH:12][CH:11]=1

Participants

4

Reactant 2

HCID 12229HydrazinecarboxaldehydeHCID 12449556HCID 12449556, compound

Product 1

HCID 12726819HCID 12726819, compound

Reagents, catalysts & solvents 1

HCID 2631-ButanolSolvent

Procedure

A mixture of 3.6 g. of 3-chloro-6-(m-fluorophenyl)pyridazine and 2.06 g. of formylhydrazine in 50 ml. of n-butanol is refluxed for 48 hr. and worked up as in Example 35 to give the product as crystals, m.p. 159°-161° C.

Workup

  1. additionA mixture of 3.6 g

Sources & evidence

ORD record
ord-facea187050c481792b467aa4f7c0a9e
Source dataset
uspto-grants-1978_09
Patent number
US04112095

Reaction notes

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