HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazinecarboxaldehyde → HCID 12726826, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazinecarboxaldehyde | HCID 12229 | — |
| Reactant | 3-Chloro-6-(2-chlorophenyl)pyridazine | HCID 12449557 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 12726826 | HCID 12726826 | — |
Reaction Steps
A mixture of 5.67 g. of 3-chloro-6-(o-chlorophenyl)pyridazine, 3.03 g. of formylhydrazine in 50 ml. of butanol is refluxed 48 hrs. to give 2.3 g. of product as pale yellow crystals, m.p. 156°-158° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04112095 |
| Source dataset | uspto-grants-1978_09 |
| ORD ID | ord-b84bde25f11c44e98d347c2957fb26f9 |
| Source note | uspto-grants-1978_09 |