Acetohydrazide → HCID 12726838, compound

HRID 1763614Notes

Reaction equation

HRID 1763614 reaction equation
Cl[C:2]1[N:3]=[N:4][C:5]([C:8]2[CH:9]=[C:10]([CH3:14])[CH:11]=[CH:12][CH:13]=2)=[CH:6][CH:7]=1.[C:15]([NH:18][NH2:19])(=O)[CH3:16]>C(O)CCC>[CH3:16][C:15]1[N:3]2[N:4]=[C:5]([C:8]3[CH:9]=[C:10]([CH3:14])[CH:11]=[CH:12][CH:13]=3)[CH:6]=[CH:7][C:2]2=[N:19][N:18]=1

Participants

4

Reactant 2

HCID 14039AcetohydrazideHCID 124495613-Chloro-6-(3-methylphenyl)pyridazine

Product 1

HCID 12726838HCID 12726838, compound

Reagents, catalysts & solvents 1

HCID 2631-ButanolSolvent

Procedure

As in Example 36, a mixture of 6.0 g. of 3-chloro-6-(m-tolyl)pyridazine and 4.34 g of acetylhydrazine in 100 ml. of n-butanol is refluxed for 48 hr. to give 2.0 g. of cream colored crystals, m.p. 160°-162° C.

Workup

  1. additionAs in Example 36, a mixture of 6.0 g
  2. customto give 2.0 g

Sources & evidence

ORD record
ord-73a53951503440678e342df4b38943ab
Source dataset
uspto-grants-1978_09
Patent number
US04112095

Reaction notes

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