Acetohydrazide → HCID 12726842, compound

HRID 1763619Notes

Reaction equation

HRID 1763619 reaction equation
Cl[C:2]1[N:3]=[N:4][C:5]([C:8]2[CH:13]=[CH:12][C:11]([Cl:14])=[C:10]([Cl:15])[CH:9]=2)=[CH:6][CH:7]=1.[C:16]([NH:19][NH2:20])(=O)[CH3:17]>C(O)CCC>[CH3:17][C:16]1[N:3]2[N:4]=[C:5]([C:8]3[CH:13]=[CH:12][C:11]([Cl:14])=[C:10]([Cl:15])[CH:9]=3)[CH:6]=[CH:7][C:2]2=[N:20][N:19]=1

Participants

4

Reactant 2

HCID 14039AcetohydrazideHCID 5985053-chloro-6-(3,4-dichlorophenyl)pyridazine

Product 1

HCID 12726842HCID 12726842, compound

Reagents, catalysts & solvents 1

HCID 2631-ButanolSolvent

Procedure

A mixture of 2.6 g. of 3-chloro-6-(3,4-dichlorophenyl)pyridazine and 1.8 g. of acetic acid hydrazide is heated in 50 ml. of n-butanol for 24 hrs. to give the product of the example.

Workup

  1. additionA mixture of 2.6 g
  2. customto give the product of the example

Sources & evidence

ORD record
ord-7a287687f93a4a8d97e51efc86d82afa
Source dataset
uspto-grants-1978_09
Patent number
US04112095

Reaction notes

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