Acetohydrazide → HCID 20310391, compound

HRID 1763620Notes

Reaction equation

HRID 1763620 reaction equation
Cl[C:2]1[N:3]=[N:4][C:5]([C:8]2[CH:13]=[C:12]([C:14]([F:17])([F:16])[F:15])[CH:11]=[CH:10][C:9]=2[Cl:18])=[CH:6][CH:7]=1.[C:19]([NH:22][NH2:23])(=O)[CH3:20]>C(O)CCC>[CH3:20][C:19]1[N:3]2[N:4]=[C:5]([C:8]3[CH:13]=[C:12]([C:14]([F:17])([F:16])[F:15])[CH:11]=[CH:10][C:9]=3[Cl:18])[CH:6]=[CH:7][C:2]2=[N:23][N:22]=1

Participants

4

Reactant 2

HCID 14039AcetohydrazideHCID 20310372HCID 20310372, compound

Product 1

HCID 20310391HCID 20310391, compound

Reagents, catalysts & solvents 1

HCID 2631-ButanolSolvent

Procedure

As in Example 36, a mixture of 2.2 g. of 3-chloro-6-[2-chloro-5-(trifluoromethyl)phenyl]pyridazine and 1.11 g. of acetylhydrazine in 50 ml. of n-butanol is refluxed for 48 hours to give the product of the example.

Workup

  1. additionAs in Example 36, a mixture of 2.2 g
  2. customto give the product of the example

Sources & evidence

ORD record
ord-6e0a7cb1902c40c2885ec480a0ac761d
Source dataset
uspto-grants-1978_09
Patent number
US04112095

Reaction notes

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