Acetohydrazide → HCID 20310383, compound

HRID 1763622Notes

Reaction equation

HRID 1763622 reaction equation
Cl[C:2]1[N:3]=[N:4][C:5]([C:8]2[CH:13]=[CH:12][C:11]([N+:14]([O-:16])=[O:15])=[C:10]([C:17]([F:20])([F:19])[F:18])[CH:9]=2)=[CH:6][CH:7]=1.[C:21]([NH:24][NH2:25])(=O)[CH3:22]>C(O)CCC>[CH3:22][C:21]1[N:3]2[N:4]=[C:5]([C:8]3[CH:13]=[CH:12][C:11]([N+:14]([O-:16])=[O:15])=[C:10]([C:17]([F:20])([F:19])[F:18])[CH:9]=3)[CH:6]=[CH:7][C:2]2=[N:25][N:24]=1

Participants

4

Reactant 2

HCID 14039AcetohydrazideHCID 20310387HCID 20310387, compound

Product 1

HCID 20310383HCID 20310383, compound

Reagents, catalysts & solvents 1

HCID 2631-ButanolSolvent

Procedure

A mixture of 4.0 g. of 3-chloro-6-[4-nitro-3-(trifluoromethyl)phenyl]pyridazine and 1.95 g. of acetylhydrazine in 40 ml. of n-butanol is refluxed for 18 hours to give the product as crystals m.p. 293°-295° C.

Workup

  1. additionA mixture of 4.0 g

Sources & evidence

ORD record
ord-4875b7ee34f741c1a612cb4d7d7eedcf
Source dataset
uspto-grants-1978_09
Patent number
US04112095

Reaction notes

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