Sodium Hydroxide → HCID 53866512, compound

HRID 1763693Notes

Reaction equation

HRID 1763693 reaction equation
C([O:4][CH:5]([CH2:28][CH2:29][CH2:30][CH2:31][CH3:32])[CH:6]=[CH:7][CH2:8][N:9]([CH2:14][CH2:15][CH2:16][C:17]1[CH:27]=[CH:26][C:20]([C:21]([O:23]CC)=[O:22])=[CH:19][CH:18]=1)[S:10]([CH3:13])(=[O:12])=[O:11])(=O)C.[OH-].[Na+]>O.CO>[OH:4][CH:5]([CH2:28][CH2:29][CH2:30][CH2:31][CH3:32])[CH:6]=[CH:7][CH2:8][N:9]([CH2:14][CH2:15][CH2:16][C:17]1[CH:27]=[CH:26][C:20]([C:21]([OH:23])=[O:22])=[CH:19][CH:18]=1)[S:10]([CH3:13])(=[O:11])=[O:12]

Participants

5

Reactant 2

HCID 14798Sodium HydroxideHCID 53672999HCID 53672999, compound

Product 1

HCID 53866512HCID 53866512, compound

Reagents, catalysts & solvents 2

HCID 887MethanolSolventHCID 962WaterSolvent

Procedure

Ethyl 4-{3-[N-(4-Acetoxy-2-nonenyl)methanesulfonamido]propyl}benzoate (23.4 g., 0.05 mole) is added to a solution of sodium hydroxide (6.0 g., 0.15 mole) in water (30 ml.) and methanol (300 ml.). The resulting solution is boiled under reflux for 2 hours.

Workup

  1. temperatureunder reflux for 2 hours

Sources & evidence

ORD record
ord-f06b1217513c45748ff45ec90fab68df
Source dataset
uspto-grants-1978_09
Patent number
US04112236

Reaction notes

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