Acetic Anhydride → 1-Chloro-4-acetoxy-8-nonene

HRID 1763696Notes

Reaction equation

HRID 1763696 reaction equation
[Cl:1][CH2:2][CH2:3][CH2:4][CH:5]([OH:11])[CH2:6][CH2:7][CH2:8][CH:9]=[CH2:10].[C:12](OC(=O)C)(=[O:14])[CH3:13]>>[Cl:1][CH2:2][CH2:3][CH2:4][CH:5]([O:11][C:12](=[O:14])[CH3:13])[CH2:6][CH2:7][CH2:8][CH:9]=[CH2:10]

Participants

3

Reactant 2

HCID 7918Acetic AnhydrideHCID 203860321-Chloro-8-nonen-4-ol

Product 1

HCID 203860741-Chloro-4-acetoxy-8-nonene

Procedure

A mixture of 1-chloro-8-nonen-4-ol (22.10 g.; 0.125 mole) and acetic anhydride (25.52 g.; 0.0250 mole) is heated on a steam bath for 1 1/2 hours.

Workup

  1. temperatureis heated on a steam bath for 1 1/2 hours

Sources & evidence

ORD record
ord-7d162e9ad8024de4bb84b0d19ed50d61
Source dataset
uspto-grants-1978_09
Patent number
US04112236

Reaction notes

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