Cadaverine → HCID 178433687, compound

HRID 1763747Notes

Reaction equation

HRID 1763747 reaction equation
[NH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][NH2:7].S([O-])([O-])(=O)=O.[CH3:13][C:14]1[NH:18][CH:17]=[N:16][C:15]=1[CH2:19][S:20][CH2:21][CH2:22][NH+:23]=[C:24]([NH2:26])S.[CH3:27][C:28]1[NH:32][CH:31]=[N:30][C:29]=1[CH2:33][S:34][CH2:35][CH2:36][NH+:37]=[C:38]([NH2:40])S>>[CH3:13][C:14]1[NH:18][CH:17]=[N:16][C:15]=1[CH2:19][S:20][CH2:21][CH2:22][N:23]=[C:24]([NH2:26])[NH:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][NH:7][C:38]([NH2:40])=[N:37][CH2:36][CH2:35][S:34][CH2:33][C:29]1[N:30]=[CH:31][NH:32][C:28]=1[CH3:27]

Participants

3

Reactant 2

HCID 273CadaverineHCID 178433692HCID 178433692, compound

Product 1

HCID 178433687HCID 178433687, compound

Procedure

The reaction of 1,5-diaminopentane (0.43 g) with S-methyl-N-[2-((5-methyl-4-imidazolyl)methylthio)ethylthiouronium sulphate (2.52 g) by the method described in Example 5 afforded the title compound which was isolated as the dipicrate (1.8 g) m.p. 115-120°.

Sources & evidence

ORD record
ord-98d7c2ec81544d3eb961a90f7ee1ad0a
Source dataset
uspto-grants-1978_09
Patent number
USRE029761

Reaction notes

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