HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-2-methoxybenzoyl chloride → HCID 20304389, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-2-methoxybenzoyl chloride | HCID 12384176 | — |
| Reactant | Ethyl 3-[4-(aminomethyl)phenyl]propanoate--hydrogen chloride (1/1) | HCID 20304428 | — |
| Product | HCID 20304389 | HCID 20304389 | — |
Reaction Steps
By reaction of ethyl β-[4-(aminomethyl)-phenyl]-propionate hydrochloride (m.p. 192°-193° C.) with 5-chloro-2-methoxybenzoyl chloride, there is obtained β-[4-(5-chloro-2-methoxybenzamidomethyl)-phenyl]-propionic acid; m.p. 152°-153° C., after recrystallization from isopropanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04113871 |
| Source dataset | uspto-grants-1978_09 |
| ORD ID | ord-65cdcfd722574cdf819d24f87418b942 |
| Source note | uspto-grants-1978_09 |