HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 11064260, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 20309081 | HCID 20309081 | — |
| Catalyst | Boron trifluoride etherate | HCID 8000 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 11064260 | HCID 11064260 | — |
Reaction Steps
Borontrifluoride etherate (5 drops) was added to a solution of the crude epoxide (9 0g) in dry benzene (250 ml). After 5 minutes water was added and the benzene layer washed with water until no longer acidic. Evaporation of solvent gave an oil which was chromatographed on silica gel; elution with progressively graded mixtures of light petroleum and ether yielded p-chlorophenyl-phenylacetaldehyde (5 68g 62%9 as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04113972 |
| Source dataset | uspto-grants-1978_09 |
| ORD ID | ord-f281c9ea5fb6405d91f419f5d4867650 |
| Source note | uspto-grants-1978_09 |