HRID1763969

反应详情

EQUATION

反应方程式

HRID 1763969 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

2-Acetoxy-3-dimethylamino- 1,1-diphenyl-propane 8200mg) was dissolved in methanolic potassium hydroxide (5% 10 ml) and the solution allowed to stand overnight. Solvent was evaporated and the residue dissolved in ether and water. The ether extract was dried and evaporated to give 3-dimethylamino-1,1- diphenyl-propan-2-ol (170 mg, 97%), m.p. 72°- 73°

WORKUP

后处理

  1. customSolvent was evaporated
  2. dissolutionthe residue dissolved in ether
  3. extractionThe ether extract
  4. customwas dried
  5. customevaporated