HRID1763969
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
2-Acetoxy-3-dimethylamino- 1,1-diphenyl-propane 8200mg) was dissolved in methanolic potassium hydroxide (5% 10 ml) and the solution allowed to stand overnight. Solvent was evaporated and the residue dissolved in ether and water. The ether extract was dried and evaporated to give 3-dimethylamino-1,1- diphenyl-propan-2-ol (170 mg, 97%), m.p. 72°- 73°
WORKUP
后处理
- customSolvent was evaporated
- dissolutionthe residue dissolved in ether
- extractionThe ether extract
- customwas dried
- customevaporated