HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4,5-Trichlorobenzenesulfonyl chloride → 2,4,5-Trichlorobenzenesulfonyl fluoride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4,5-Trichlorobenzenesulfonyl chloride | HCID 27575 | — |
| Reactant | Potassium Fluoride | HCID 522689 | — |
| Product | 2,4,5-Trichlorobenzenesulfonyl fluoride | HCID 20511726 | 99% |
Reaction Steps
2,4,5-Trichlorobenzenesulfonyl fluoride was synthesized from potassium fluoride and 2,4,5-trichlorobenzenesulfonyl chloride using the procedure described in Example 1. A product with mp 80°-83° C was obtained in 99% yield. The chemical analysis, NMR and IR spectra were in agreement with the assigned structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04115059 |
| Source dataset | uspto-grants-1978_09 |
| ORD ID | ord-c6cc9c6cc38b44a593ddd35998180d7c |
| Source note | uspto-grants-1978_09 |