1-(2,6-Dimethylphenyl)-3-methylguanidine hydrochloride → HCID 178485094, Verbindung

HRID 1764195Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1764195
Cl.[CH3:2][C:3]1[CH:8]=[CH:7][CH:6]=[C:5]([CH3:9])[C:4]=1[NH:10][C:11]([NH:13][CH3:14])=[NH:12]>[OH-].[Na+]>[CH3:9][C:5]1[CH:6]=[CH:7][CH:8]=[C:3]([CH3:2])[C:4]=1[NH:10][C:11]([NH:13][CH3:14])=[NH:12]

Komponenten

3

Edukt 1

HCID 1784850951-(2,6-Dimethylphenyl)-3-methylguanidine hydrochloride

Produkt 1

HCID 178485094HCID 178485094, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 14798Sodium HydroxideLösungsmittel

Versuchsvorschrift

The free base is prepared by dissolving 1-(2,6-dimethylphenyl)-3-methylguanidine hydrochloride in 10% sodium hydroxide solution and extracting with ether. The ether is dried and evaporated to dryness to obtain 1-(2,6-dimethylphenyl)-3-methylguanidine.

Aufarbeitung

  1. customThe free base is prepared
  2. extractionextracting with ether
  3. dry with materialThe ether is dried
  4. customevaporated to dryness

Quellen und Nachweise

ORD-Eintrag
ord-f03fe7e611994b87a57fac300b4fc56a
Quelldatensatz
uspto-grants-1978_09
Patentnummer
US04115564

Notizen zur Reaktion

Wird geladen…