4-Chloro-10H-phenoxazine → HCID 20307142, compound

HRID 1764227Notes

Reaction equation

HRID 1764227 reaction equation
[Cl:1][C:2]1[C:15]2[O:14][C:13]3[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=3)[NH:7][C:6]=2[CH:5]=[CH:4][CH:3]=1.Cl.Cl[C:18]1[N:19]([C:23]2[CH2:27][CH2:26][CH2:25][N:24]=2)[CH2:20][CH2:21][CH:22]=1>>[ClH:1].[Cl:1][C:2]1[C:15]2[O:14][C:13]3[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=3)[N:7]([C:18]3[N:19]([C:23]4[CH2:27][CH2:26][CH2:25][N:24]=4)[CH2:20][CH2:21][CH:22]=3)[C:6]=2[CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 143402424-Chloro-10H-phenoxazineHCID 203071382-Chloro-1-(1-pyrrolin-2-yl) 2-pyrroline hydrochloride

Product 1

HCID 20307142HCID 20307142, compound

Procedure

Reaction of 4-chlorophenoxazine with 2-chloro-(1-pyrrolin-2-yl)pyrroline hydrochloride according to the procedure of Example 7 affords 4-CHLORO-10-[1-(1-PYRROLIN-2-YL)-2-PYRROLIN-2-YL]PHENOXAZINE HYDROCHLORIDE, m.p. 278°-282° C. (dec.), from ethanol-ether.

Sources & evidence

ORD record
ord-4dac89d628d04f128990f631c1bf3f40
Source dataset
uspto-grants-1978_09
Patent number
US04115571

Reaction notes

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