HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Difluoronitrobenzene → Methyl 5-methyl-2-(2-nitro-4-fluoroanilino)-thiophene-3-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Difluoronitrobenzene | HCID 67767 | — |
| Reactant | Methyl-2-amino-5-methyl-3-thiophenecarboxylate | HCID 675878 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Methyl 5-methyl-2-(2-nitro-4-fluoroanilino)-thiophene-3-carboxylate | HCID 20387797 | — |
Reaction Steps
Methyl 2-amino-5-methyl-thiophene-3-carboxylate and 2,5-difluoronitrobenzene, m.p. 149°-151° C. (EtOH).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04115568 |
| Source dataset | uspto-grants-1978_09 |
| ORD ID | ord-daa9b48f2fc34916b9ed5c2f5bbf1ada |
| Source note | uspto-grants-1978_09 |