1H-Imidazole, 1-[2-(2,4-dichlorophenyl)hexyl]- → HCID 70588101, compound

HRID 1764292Notes

Reaction equation

HRID 1764292 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[CH:9]([CH2:16][CH2:17][CH2:18][CH3:19])[CH2:10][N:11]1[CH:15]=[CH:14][N:13]=[CH:12]1>CCOCC>[ClH:1].[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[CH:9]([CH2:16][CH2:17][CH2:18][CH3:19])[CH2:10][N:11]1[CH:15]=[CH:14][N:13]=[CH:12]1

Participants

3

Reactant 1

HCID 30068521H-Imidazole, 1-[2-(2,4-dichlorophenyl)hexyl]-

Product 1

HCID 70588101HCID 70588101, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

In 30.0 g (0.101 mole) of 1-[β-(2,4-dichlorophenyl)hexyl]imidazole dissolved in 200 ml of ether is bubbled dry hydrogen chloride gas until the mixture is acidic to litmus. A colorless solid forms which is separated by filtration to give 24.5 g. of the hydrochloride salt which is identified by nmr.

Workup

  1. customis bubbled dry hydrogen chloride gas until the mixture
  2. customA colorless solid forms which is separated by filtration
  3. customto give 24.5 g

Sources & evidence

ORD record
ord-45468025b3d84f2f85252110a5ae5150
Source dataset
uspto-grants-1978_09
Patent number
US04115578

Reaction notes

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