HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → HCID 20306117, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Nitric acid--1-{2-[4-(methylsulfanyl)phenyl]hexyl}-1H-imidazole (1/1) | HCID 20306129 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 20306117 | HCID 20306117 | — |
Reaction Steps
To 7.0g (0.021 mole) of 1-[β-(p-methylthiophenyl) hexyl]imidazole nitric acid salt in 75 ml of glacial acetic acid is added dropwise at less than 10°, 8.0g (0.083 mole) of 35% hydrogen peroxide. When the addition is complete, the reaction is stirred for 1 hour heated on a steambath for a second hour and then poured into iced water. The solution is made basic to litmus with sodium hydroxide and the product is extracted out with ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04115578 |
| Source dataset | uspto-grants-1978_09 |
| ORD ID | ord-c7077014c61245f0a16459c77e55e9e8 |
| Source note | uspto-grants-1978_09 |