Methyl iodide → HCID 22768153, compound

HRID 1764407Notes

Reaction equation

HRID 1764407 reaction equation
[CH2:1]([N:3]([CH2:16][CH2:17][CH2:18][CH3:19])[C:4]([NH:6][C:7]1[CH:11]=[C:10]([C:12]([CH3:15])([CH3:14])[CH3:13])[O:9][N:8]=1)=[O:5])[CH3:2].[CH3:20]I>>[CH2:1]([N:3]([CH2:16][CH2:17][CH2:18][CH3:19])[C:4]([N:6]([CH3:20])[C:7]1[CH:11]=[C:10]([C:12]([CH3:13])([CH3:15])[CH3:14])[O:9][N:8]=1)=[O:5])[CH3:2]

Participants

3

Reactant 2

HCID 6328Methyl iodideHCID 22768165N-Butyl-N'-(5-tert-butyl-1,2-oxazol-3-yl)-N-ethylurea

Product 1

HCID 22768153HCID 22768153, compound

Procedure

The reaction is effected as in Example 171 by using 1-ethyl-1-butyl-3-(5-t-butyl-3-isoxazolyl)urea and methyl iodide to give 1-ethyl-1-butyl-3-methyl-3-(5-t-butyl-3-isoxazolyl)urea as an oil boiling at 140° to 145° C (bath temperature)/0.67 mm Hg.

Sources & evidence

ORD record
ord-5ce9c5e6a87046ba91a4dd17971ef134
Source dataset
uspto-grants-1978_09
Patent number
US04116671

Reaction notes

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