HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazinecarboxaldehyde → 6-(p-Bromophenyl)-1,2,4-triazolo[4,3-b]pyridazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazinecarboxaldehyde | HCID 12229 | — |
| Reactant | 3-(4-Bromophenyl)-6-chloropyridazine | HCID 6405255 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | 6-(p-Bromophenyl)-1,2,4-triazolo[4,3-b]pyridazine | HCID 22768933 | — |
Reaction Steps
A mixture of 3.76 g. of 3-(p-bromophenyl)-6-chloropyridazine, 1.80 g. of formylhydrazine and 50 ml. of butyl alcohol is heated to reflux and allowed to reflux overnight. The reaction mixture is allowed to cool and the precipitated product is washed with water, air dried and recrystallized from methyl alcohol, m.p. 209°-211° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04117130 |
| Source dataset | uspto-grants-1978_09 |
| ORD ID | ord-75431e61e93e4b2a95d18a4233c3c94c |
| Source note | uspto-grants-1978_09 |