HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 178487596, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 178487594 | HCID 178487594 | — |
| Reactant | HCID 178487598 | HCID 178487598 | — |
| Solvent | Thionyl Chloride | HCID 24386 | — |
| Product | HCID 178487596 | HCID 178487596 | — |
Reaction Steps
N2 (6-methoxy-2-naphthylsulfonyl)-L-arginyl chloride. A suspension of 2.5 g of N2 -(6-methoxy-2-naphthylsulfonyl)-L-arginine in 20 ml of thionyl chloride was stirred for 2 hours at room temperature. Addition of cold dry ethyl ether resulted in a precipitate which was collected by filtration and washed several times with dry ethyl ether to give N2 -(6-methoxy-2-naphthylsulfonyl)-L-arginyl chloride. (B) Ethyl 1-[N2 -(6-methoxy-2-naphthylsulfonyl)-L-arginyl]-2-piperidinecarboxylate
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04117127 |
| Source dataset | uspto-grants-1978_09 |
| ORD ID | ord-9df9d19da3084cea908562e2f7848054 |
| Source note | uspto-grants-1978_09 |