HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 178495937, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 178495947 | HCID 178495947 | — |
| Product | HCID 178495937 | HCID 178495937 | — |
Reaction Steps
A suspension of 2.00 g of N2 -(6,7-dimethoxy-2-naphthylsulfonyl)-L-arginyl-N-(2-methoxyethyl)glycine in 20 ml of thionyl chloride was stirred for 2 hours at room temperature. Addition of cold dry ethyl ether resulted in a precipitate which was collected by filtration and washed several times with dry ethyl ether to give N2 -(6,7-dimethoxy-2-naphthylsulfonyl)-L-arginyl-N-(2-methoxyethyl)glycyl chloride hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04117127 |
| Source dataset | uspto-grants-1978_09 |
| ORD ID | ord-d7435c4337fa4d5cbe172f77c2f49528 |
| Source note | uspto-grants-1978_09 |