HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydrazinylbenzenesulfonamide hydrochloride → HCID 9864112, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydrazinylbenzenesulfonamide hydrochloride | HCID 2794567 | — |
| Reactant | 3-Buten-2-one,1,1,1-trifluoro-4-phenyl- | HCID 6006052 | — |
| Product | HCID 9864112 | HCID 9864112 | 73% |
Reaction Steps
A solution of trans-1,1,1-trifluoro-4-phenyl-3-buten-2-one (5 mmol) and 4-sulfamylphenyl hydrazine hydrochloride (6 mmol) was subjected to Procedure 3. The title compound was obtained in 73% yield, m.p. 178-180° C.; C, H analysis (C18H15SO2N4F3.H2O):
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE039681E1 |
| Source dataset | uspto-grants-2007_06 |
| ORD ID | ord-684a1471cb6349b7982e2f11a193ac2d |
| Source note | uspto-grants-2007_06 |