HCID 178418361, compound → HCID 178450440, compound

Participants

Reaction Steps

To 20 g of 5-(3-hydroxy-1-hexynyl)-2,3,4-trifluoro-1-[trans-4-(trans-4-propylcyclohexyl) cyclohexyl]benzene which was dissolved into 80 mL of ethanol, 2 g of 5% palladium carbon (50% in water) was added, stirred for 6 hours at a hydrogen pressure of 0.5 MPa, and was then left to stand overnight. After palladium carbon was removed by filtration, the solvent was evaporated under a reduced pressure to obtain 10 g of 5-(3-hydroxy-1-hexyl)-2,3,4-trifluoro-1-[trans-4-(trans-4-propylcyclohexyl)cyclohexyl]benzene.

Provenance & Evidence