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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1765014Generated: October 29, 2026

Methyl p-toluenesulfonate → HCID 178503586, compound

https://huagongshe.com/reaction/1765014

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl p-toluenesulfonateHCID 6645—
ReactantHCID 11263876HCID 11263876—
SolventEthyl AcetateHCID 8857—
ProductHCID 178503586HCID 178503586—

Reaction Conditions

Temperature120 °C

Reaction Steps

A mixture of 0.127 g of 2-methylthiothiazolo[5,4-c]pyridine (from methylation of thiazolo[5,4-c]pyridine-2(1H)-thione with potassium carbonate and methyl iodide) and 0.143 g methyl tosylate is heated at 120° C. for one hour. Ethyl acetate (8 mL) is added, the mixture is stirred for 30 minutes, and Compound 6 is isolated by suction filtration.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07226740B2
Source datasetuspto-grants-2007_06
ORD IDord-40f69f689bab4b4fa3a77d92f266fc5a
Source noteuspto-grants-2007_06