3-Biphenylamine, 3'-nitro- → HCID 22732389, compound

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The title compound was prepared from a mixture of 4-chloro-2-(3-pyridinyl)-6-(trifluoromethyl)pyrimidine (50 mg, 0.193 mmol) and 3-amino-3′-nitrobiphenyl (83 mg, 0.386 mmol) similar to Example 58 and isolated as a light tan solid (65 mg, 77%). 1H NMR (DMSO-d6): 13.00 (s, 1H), 11.94 (s, 1H), 11.23 (d, J=4.5 Hz, 1H), 11.11 (d, J=8.1 Hz, 1H), 10.97 (s, 1H), 10.78 (s, 1H), 10.75 (s, 1H), 10.69 (d, J=8.1 Hz, 1H), 10.35–10.28 (m, 2H), 10.14–10.04 (m, 3H), 9.67 (s, 1H).

Provenance & Evidence